MXene have gather massive attention in the last decades owing their physical chemical properties. However, their synthesis requires the use of hazardous chemicals, delaying their integration in industry.
In this work we propose electrochemical synthesis as a pathway to address the sustainability of mxenes. We surpass the state of the art by exploring pulsed voltammetry as a method to secure high yield and high quality mxene. The pulses of voltage generate nanobubbles at the MAX interface, cleaning it from MXene and byproduct, namely reactivating its electrochemical activity.